Chapter 4 efficiency of columns free download as powerpoint presentation. Pdf resume of the extension of the ponchon and savarit. A revision of the distillation theory is presented in this paper which is free from such weaknesses. The number of theoretical stages for an operating reflux ratio of r l0d 2. Welcome to the twelfth lecture of module 5 on mass transfer. These methods are based on the geometrical concepts of the ponchon and savarit method for binary systems and use the geometrical conditions. Its one of the blackboxes which appeared in process and performs some physical as opposed to chemical change. Fractional distillation using the saturated liquid enthalpy. Fractional distillation using enthalpyconcentration method.
Nihad omer hassan 2 course description 2 hours lecture, 2 hour tutorial per week, 3 credit hours. Upload document file or like to download immediately close. Distillation with non constant molar overflow lewis method 1. In the ponchonsavarit diagram, the reactive cascade difference point has two elements. Working on the hx diagram is more general than a mccabethiele construction, because it takes direct account of the thermal effects and does not require an assumption of equimolal overflow. However, it is demonstrated that there are a number of weaknesses in this method when it is. Consider the distillation of a binary mixture in a con ventional column with a. Ponchonsavarit method for binary distillation che 2 leadlearn report batenga. One is the composition coordi nate formed as a linear combination of. May 30, 2016 calculation of number of trays for a distillation column is illustrated using the ponchonsavarits method using the enthalpy diagram for saturated vapor enthalpy curve versus y and saturated. As is often the case in chemical processing, analytical calculations are simplified for binary systems, and a graphical solution is possible on an enthalpy.
The ponchonsavarit graphical construction allows the determination of the number of equilibrium stages in the case of the separation of a binary mixture composed of hexane and octane. A revision of the distillation theory jinlun wang1 and g. Ponchon savarit distillation system buffalo brewing blog. Resume of the extension of the ponchon and savarit method for designing ternary rectification columns 334 ponchonsavarit method to reactive distillation, minimum reflux ratio calculation and quaternary liquidliquid extractors, respectively. Ponchon savarit method pdf this approach is sometimes called the ponchonsavarit method. Fractionation is a multistage countercurrent distillation operation.
Pdf this work presents a summary of the analytical extension of the classical ponchon and savarit method for the design of binary distillation. Analysis of binary distillation by ponchon savarit method. Resume of the extension of the ponchon and savarit method for designing ternary rectification columns 1934 e once the coefficients of the 4 parabolas have been obtained, the points pm,5 of the. There are several ways of incorporating the energy effects. Resume of the extension of the ponchon and savarit method for designing ternary rectification columns 1934 e once the coefficients of the 4 parabolas have been obtained, the points pm,5 of. Modified ponchonsavarit and mccabethiele methods for. So, equimolal overflow which we have assumed for the. Fractional distillation using enthalpyconcentration method so molal flow rates need not to be constant using enthalpy as well as material balances when the operating lines are plotted with the equilibrium curve on the xy diagram, the mccabethiele stepbystep construction can be used to compute the number of ideal plates. Ponchon savarit is a classical graphical method for the design of binary distillation columns. This approach is sometimes called the ponchonsavarit method.
Your text does not include this method, but it may be useful. The construction for a partial condenser with both a vapor and liquid product is shown in fig. Calculation of number of trays for a distillation column is illustrated using the ponchonsavarits method using the enthalpy diagram for saturated vapor enthalpy curve versus y and saturated. Ali mansoori2 abstract the mccabethiele graphical method is considered as a basic and simple technique to determine the number of theoretical stages in a distillation column.
Analysis of the zone connecting consecutive sectors in. This graphical method uses both material and energy balances to determine the number of theoretical stages required to achieve a specific separation. The method is concerned with the graphical analysis of calculating the theoretical stages by enthalpy balance required for desired separation by distillation process hines and maddox, 1984. New methods for orienting the calculation of the minimum reflux ratio for distillation columns have been developed. A graphical method for designing reactive distillation columns ithe ponchon savarit method article in proceedings of the royal society a 4562000.
Modified ponchon savarit and mccabethiele methods for free download as pdf file. This demonstration displays the number of equilibrium stages for the total reflux case. Graphical construction is done on the enthalpy composition diagram. For multistage tray towers ponchon savarit method was first developed for the case of negligible heat losses. Two simulators for the ponchonsavarit distillation process have been developed, one using simple binary rectification, and the second using opensteam binary rectification processes. We first show the properties needed for points to lie on a straight line in compositionenthalpy space. Mccabe thiele method of design of distillation column their rates are independent of the. Ponchonsavarit graphical method at total reflux wolfram. Tutorial on the use of ponchon savarits method for.
Sep 03, 2018 binary distillation using mccabethiele graphical method pdf. Textbooks applied process design for chemical and petrochemical plants, ernest e. Savarit method for graphically analyzing and designing internally heatintegrated distillation columns. It is not the intention of this publication to discuss methods for calculating a distillation system. Though different in the mathematical formulation of the stripping zone, they have the same method of coding. This method is still widely used, mainly with didactical purposes, though it. A distillation column operating at 1 atm is to be designed for separating an ethanolwater mixture. Additionally, the use of topological analysis has been applied with success in the design of. The very shape of the hx diagram provides a clue as to the importance of the energy. Numerical simulations research for applications in binary. The use of the method is illustrated in the case studies. This approach is sometimes called the ponchon savarit method.
Continuous distillation ponchon savarit method for the same question in tutorial 5, use the ponchon savarit method to determine the total number of theoretical plates required. The ponchonsavarit method for binary systems in distillation, energy effects are significant, as materials are being vaporized and condensed. Classical graphical calculations have been the mccabethiele method, using the data shown in figure 2, and the ponchon savarit method, which is more accurate and uses an enthalpy diagram, as shown in figure 3, as well as the vle data. A graphical method for designing reactive distillation. Savarit method, which includes the energy balance, in this study, a graphical hidic design procedure using hxy diagrams is also proposed. Apr 21, 2015 a revision of the distillation theory part i 20171002. Ponchon savarit method for design of binary distillation column kghr of a mixture containing 42 mole percent heptane and 58 mole percent ethyl benzene is to be fractionated to a distillate containing 97 mole percent heptane and a residue containing 99 mole percent ethyl benzene using a total condenser and feed at its saturated liquid condition. A graphical method for designing reactive distillation columns. Distillation is continued, either until the residue of the still contains a material with an acceptably low content of the volatile material, or until the distillate is no longer suf.
The ponchon savarit method for binary systems in distillation. The mccabethoole method is considered to be the simplest and perhaps most instructive method for the analysis of binary distillation. View lab report ponchonsavarit graphical method ppt. The ponchon savarit graphical construction allows the rigorous computation of the number of equilibrium stages in the case of the separation of a binary mixture composed of hexane and octane.
A unit operation is one step in a process to convert a raw material into some useful chemical product. Tutorial on the use of ponchon savarits method for distillation. Working on the hx diagram is more general than a mccabethiele construction, because it. The ponchon savarit method is a graphical approach that does not require an assumption of equimolal overflow. Recalculate the number of theoretical stages required. We show how to construct a ponchon savarit diagram for a binary reactive distillation column, illustrating it specifically for isomerization and decomposition reactions. Binary distillation using mccabethiele graphical method pdf. A revision of the distillation theory part i 20171002. Pdf resume of the extension of the ponchon and savarit method. Mccabethele method, determination of the stripping section operating line sol, analysis of binary distillation by ponchon savarit method. Abstract this paper presents a series of calculation procedures for computer design of ternary distillation columns overcoming the iterative equilibrium calculations necessary in these kind of problems and, thus, reducing the calculation time. Distillation calculations can be performed graphically on an enthalpyconcentration hx diagram. Analysis of binary distillation by ponchonsavarit method background principle. It is demonstrated that this revised distillation theory is applicable to graphical binary distillation as well as to the analytical stagetostage calculation method, the ponchon savarit method and the shortcut approximate method of binary.
Ponchonsavarit graphical equilibrium stage method wolfram. Jun 22, 2012 distillation with non constant molar overflow lewis method 1. Distillation is the process of separation and purification of different components of mixture of two or more organic liquids with appreciable. Fractional distillation ponchon savarit and mccabe thiele.
Jul 26, 2016 lecture 1 distillation introduction 1. Fractional distillation ponchon savarit and mccabe thiele methods. Week 7 mccabethiele method binary distillation process on xy diagram, operating and equilibrium lines week 8 mccabethiele method feed conditions, stepping off stages, limiting conditions minimum reflux, minimum number of stages, murphree and overall efficiency week 9 ponchon savarit method how to prepare enthalpy diagram hxy. Introduction nihad omer hassan 1nihad omer hassan 2.
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